If I've said it once, I've said it a million times, but Eye of the Beholder is incredibly effective. Although fairly obvious when watching, it never fails to work for a first time viewer.
Another one I really like is The Rip Van Winkler Case. The four men put so much work into making sure that gold was worth something to them, that they didn't think about the world around them.
The Silence is also a really good "twist" episode.
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